2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine

Base Information

• Chemical Name: 2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine
• CAS No.: 75802-08-3
• Molecular Formula: C₁₅H₂₂N₂O₂S
• Molecular Weight: 294.418
• Mol file: 75802-08-3.mol

Synonyms:2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine

Chemical Property of 2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine

There total 1 articles about 2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

1-ethyl-3,3-pentamethylenediaziridine (52551-68-5) + p-toluenesulfonyl chloride (98-59-9) → 2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine (75802-08-3)

Guidance literature:

With triethylamine; for 3.5h;

DOI:10.1021/jo00315a019

Reference yield: 85.0%

2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine (75802-08-3) + phenyl isocyanate (103-71-9) → 1-Ethyl-2-(p-toluenesulfonyl)-4-phenyl-5,5-pentamethylene-1,2,4-triazolidin-3-one (75802-12-9)

Guidance literature:

at 90 ℃; for 3h;

DOI:10.1021/jo00315a019

Reference yield: 82.0%

2-Ethyl-1-(p-toluenesulfonyl)-3,3-pentamethylenediaziridine (75802-08-3) + benzoyl isocyanate (4461-33-0) → 1-Ethyl-2-(p-toluenesulfonyl)-4-benzoyl-5,5-pentamethylene-1,2,4-triazolidin-3-one (75802-16-3)

Guidance literature:

In benzene; at 70 ℃; for 2h;

DOI:10.1021/jo00315a019

upstream raw materials:

1-ethyl-3,3-pentamethylenediaziridine

p-toluenesulfonyl chloride

Downstream raw materials:

1-Ethyl-2-(p-toluenesulfonyl)-4-phenyl-5,5-pentamethylene-1,2,4-triazolidin-3-one

1-Ethyl-2-(p-toluenesulfonyl)-4-(1-naphthyl)-5,5-pentamethylene-1,2,4-triazolidin-3-one

1-Ethyl-2-(p-toluenesulfonyl)-4-benzoyl-5,5-pentamethylene-1,2,4-triazolidin-3-one