C₁₄H₂₂O₂

Base Information

Chemical Name:C₁₄H₂₂O₂
CAS No.:1454916-00-7
Molecular Formula:C₁₄H₂₂O₂
Molecular Weight:222.327
Hs Code.:

C<sub>14</sub>H<sub>22</sub>O<sub>2</sub>

Synonyms:C₁₄H₂₂O₂

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Chemical Property of C₁₄H₂₂O₂

Chemical Property:

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Technology Process of C₁₄H₂₂O₂

There total 7 articles about C₁₄H₂₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₄₄O₂Si₂

: 1454916-00-7
C₁₄H₂₂O₂

: 1454916-01-8
C₁₄H₂₂O₂

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c3cc45170d

Reference yield:

: 1454915-72-0
ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate

: 1454916-00-7
C₁₄H₂₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: L-Selectride / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / toluene / 0.67 h / -78 °C / Inert atmosphere

4.2: Na/K tartrate / 2 h / 20 °C / Inert atmosphere

5.1: ethynylmagnesium chloride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium tetrahydroborate; ethynylmagnesium chloride; tetrabutyl ammonium fluoride; L-Selectride; diisobutylaluminium hydride; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1039/c3cc45170d

Reference yield:

: 1454915-98-0
C₁₇H₃₂O₃Si

: 1454916-00-7
C₁₄H₂₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / toluene / 0.67 h / -78 °C / Inert atmosphere

1.2: Na/K tartrate / 2 h / 20 °C / Inert atmosphere

2.1: ethynylmagnesium chloride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

With ethynylmagnesium chloride; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; In tetrahydrofuran; toluene;
DOI:10.1039/c3cc45170d