ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate

Base Information

• Chemical Name: ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate
• CAS No.: 1454915-72-0
• Molecular Formula: C₁₄H₂₀O₃
• Molecular Weight: 236.311

Synonyms:ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate

Chemical Property of ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate

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Technology Process of ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate

There total 1 articles about ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(S)-p-mentha-6,8-dien-2-one (2244-16-8,6485-40-1) + ethyl bromoacetate (105-36-2) → ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate (1454915-72-0)

Guidance literature:

(S)-p-mentha-6,8-dien-2-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

ethyl bromoacetate; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1039/c3cc45170d

Reference yield: 79.0%

ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate (1454915-72-0) → ethyl 2-((1R,2S,6S)-2-hydroxy-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate (1454915-73-1)

Guidance literature:

With sodium tetrahydroborate; cerium(III) chloride heptahydrate; In methanol; at -78 - -30 ℃; Inert atmosphere;

DOI:10.1039/c3cc45170d

Reference yield: 60.0%

ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate (1454915-72-0) → C14H22O3 (1454915-96-8)

Guidance literature:

With L-Selectride; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c3cc45170d

upstream raw materials:

(S)-p-mentha-6,8-dien-2-one

ethyl bromoacetate

Downstream raw materials:

C₁₆H₂₂O₃

C₁₉H₃₀O₃Si

C₁₉H₂₈O₃

C₂₂H₃₆O₃Si

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