1>-AM-toxin

Base Information

Chemical Name:1>-AM-toxin
CAS No.:60008-08-4
Molecular Formula:C₂₁H₂₇N₃O₆
Molecular Weight:417.462
Hs Code.:

Synonyms:1>-AM-toxin

Suppliers and Price of 1>-AM-toxin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1>-AM-toxin

Chemical Property:

Purity/Quality:

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Technology Process of 1>-AM-toxin

There total 11 articles about 1>-AM-toxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 78700-31-9
[12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide

: 60008-08-4
1>-AM-toxin

Guidance literature:: With potassium hydrogencarbonate; In ethyl acetate; at 70 ℃; for 5h;
DOI:10.1016/S0040-4039(01)81977-8

Reference yield:

: 4026-18-0,17407-55-5,17407-56-6,600-37-3
2-hydroxy-3-methylbutanoic acid

: 60008-08-4
1>-AM-toxin

Guidance literature:: Multi-step reaction with 11 steps

2: EDC

4: 83 percent / HCl / dioxane

5: 82 percent

6: EDC / dimethylformamide

7: trifluoroacetic acid

8: pyridine / 48 h / Ambient temperature

9: H₂ / Pd / HCl; dimethylformamide

10: KHCO₃ / ethyl acetate / 144 h

11: 24 percent / KHCO₃ / ethyl acetate / 5 h / 70 °C

With hydrogenchloride; hydrogen; potassium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; palladium; In 1,4-dioxane; pyridine; hydrogenchloride; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81977-8

Reference yield:

: 65096-39-1,112037-09-9
Boc-L-Ala-L-Hmb-ONSu

: 60008-08-4
1>-AM-toxin

Guidance literature:: Multi-step reaction with 9 steps

2: 83 percent / HCl / dioxane

3: 82 percent

4: EDC / dimethylformamide

5: trifluoroacetic acid

6: pyridine / 48 h / Ambient temperature

7: H₂ / Pd / HCl; dimethylformamide

8: KHCO₃ / ethyl acetate / 144 h

9: 24 percent / KHCO₃ / ethyl acetate / 5 h / 70 °C

With hydrogenchloride; hydrogen; potassium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; palladium; In 1,4-dioxane; pyridine; hydrogenchloride; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81977-8