[12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide

Base Information

Chemical Name:[12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide
CAS No.:78700-31-9
Molecular Formula:C₂₄H₃₇N₄O₆*I
Molecular Weight:604.485
Hs Code.:

Synonyms:[12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide

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Chemical Property of [12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide

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Technology Process of [12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide

There total 10 articles about [12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4026-18-0,17407-55-5,17407-56-6,600-37-3
2-hydroxy-3-methylbutanoic acid

: 78700-31-9
[12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 10 steps

2: EDC

4: 83 percent / HCl / dioxane

5: 82 percent

6: EDC / dimethylformamide

7: trifluoroacetic acid

8: pyridine / 48 h / Ambient temperature

9: H₂ / Pd / HCl; dimethylformamide

10: KHCO₃ / ethyl acetate / 144 h

With hydrogenchloride; hydrogen; potassium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; palladium; In 1,4-dioxane; pyridine; hydrogenchloride; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81977-8

Reference yield:

: 65096-39-1,112037-09-9
Boc-L-Ala-L-Hmb-ONSu

: 78700-31-9
[12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 8 steps

2: 83 percent / HCl / dioxane

3: 82 percent

4: EDC / dimethylformamide

5: trifluoroacetic acid

6: pyridine / 48 h / Ambient temperature

7: H₂ / Pd / HCl; dimethylformamide

8: KHCO₃ / ethyl acetate / 144 h

With hydrogenchloride; hydrogen; potassium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; palladium; In 1,4-dioxane; pyridine; hydrogenchloride; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81977-8

Reference yield:

: 78700-15-9
(S)-2-[(S)-2-((S)-2-tert-Butoxycarbonylamino-propionyloxy)-3-methyl-butyrylamino]-3-(4-methoxy-phenyl)-propionic acid

: 78700-31-9
[12-Isopropyl-9-(4-methoxy-benzyl)-3-methyl-2,5,8,11-tetraoxo-1-oxa-4,7,10-triaza-cyclododec-6-ylmethyl]-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 7 steps

1: 83 percent / HCl / dioxane

2: 82 percent

3: EDC / dimethylformamide

4: trifluoroacetic acid

5: pyridine / 48 h / Ambient temperature

6: H₂ / Pd / HCl; dimethylformamide

7: KHCO₃ / ethyl acetate / 144 h

With hydrogenchloride; hydrogen; potassium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; palladium; In 1,4-dioxane; pyridine; hydrogenchloride; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81977-8