(2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone

Base Information

Chemical Name:(2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone
CAS No.:1393834-11-1
Molecular Formula:C₃₃H₃₁NO₄
Molecular Weight:505.613
Hs Code.:

Synonyms:(2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone

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Chemical Property of (2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone

Chemical Property:

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Technology Process of (2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone

There total 4 articles about (2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1393833-94-7
(2'R,4R,Z)-N-(4'-benzyloxyl-2-methylbut-3'-enoyl)-4,5,5-triphenyloxazolidin-2-one

: 1393834-11-1
(2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethanol; at 25 ℃; for 16h;
DOI:10.1016/j.tetlet.2012.06.133

Reference yield:

: 363165-99-5
4-(benzyloxyl)-but-2-enoic acid

: 1393834-11-1
(2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1.1: pivaloyl chloride / tetrahydrofuran / 18 h / 0 - 25 °C

2.1: potassium hexamethylsilazane; lithium chloride / tetrahydrofuran / 0.5 h / -60 °C / Inert atmosphere

2.2: 7 h / -60 - -45 °C / Inert atmosphere

2.3: Inert atmosphere; Saturated solution

3.1: palladium on activated charcoal; hydrogen / ethanol / 16 h / 25 °C

With palladium on activated charcoal; hydrogen; pivaloyl chloride; potassium hexamethylsilazane; lithium chloride; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tetlet.2012.06.133

Reference yield:

: C₃₂H₂₇NO₄

: 1393834-11-1
(2'R,4R)-3-(4'-benzyloxy-2'-methylbutanoyl)-4,5,5-triphenyloxazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylsilazane; lithium chloride / tetrahydrofuran / 0.5 h / -60 °C / Inert atmosphere

1.2: 7 h / -60 - -45 °C / Inert atmosphere

1.3: Inert atmosphere; Saturated solution

2.1: palladium on activated charcoal; hydrogen / ethanol / 16 h / 25 °C

With palladium on activated charcoal; hydrogen; potassium hexamethylsilazane; lithium chloride; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tetlet.2012.06.133