5-Bromo-3,4-dimethylbenzene-1,2-diamine

Base Information

Chemical Name:5-Bromo-3,4-dimethylbenzene-1,2-diamine
CAS No.:107100-16-3
Molecular Formula:C8H11 Br N2
Molecular Weight:215.093
Hs Code.:2921590090
DSSTox Substance ID:DTXSID70379134
Wikidata:Q82168803
Mol file:107100-16-3.mol

Synonyms:5-bromo-3,4-dimethylbenzene-1,2-diamine;107100-16-3;5-Bromo-1,2-diamino-3,4-dimethylbenzene;1,2-Benzenediamine,5-bromo-3,4-dimethyl-;SCHEMBL703842;DTXSID70379134;VVZQTDJQVSDRAY-UHFFFAOYSA-N;MFCD00052696;AKOS015912372;PS-4162;SB77006;BP-10133;5-bromo-3,4-dimethyl-benzene-1,2-diamine;5-Bromo-2-(dimethylamino)-6-methylpyridine;CS-0314347;FT-0620115;A801582;W-204622

Suppliers and Price of 5-Bromo-3,4-dimethylbenzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Bromo-3,4-dimethylbenzene-1,2-diamine
500mg
$ 130.00

TRC
5-Bromo-3,4-dimethylbenzene-1,2-diamine
100mg
$ 60.00

SynQuest Laboratories
5-Bromo-3,4-dimethylbenzene-1,2-diamine
250 mg
$ 36.00

SynQuest Laboratories
5-Bromo-3,4-dimethylbenzene-1,2-diamine
1 g
$ 104.00

SynQuest Laboratories
5-Bromo-3,4-dimethylbenzene-1,2-diamine
5 g
$ 312.00

Crysdot
5-Bromo-3,4-dimethylbenzene-1,2-diamine 97%
10g
$ 341.00

Biosynth Carbosynth
5-Bromo-3,4-dimethylbenzene-1,2-diamine
2 g
$ 360.00

Biosynth Carbosynth
5-Bromo-3,4-dimethylbenzene-1,2-diamine
5 g
$ 780.00

Biosynth Carbosynth
5-Bromo-3,4-dimethylbenzene-1,2-diamine
1 g
$ 220.00

Biosynth Carbosynth
5-Bromo-3,4-dimethylbenzene-1,2-diamine
500 mg
$ 140.00

Total 19 raw suppliers

Chemical Property of 5-Bromo-3,4-dimethylbenzene-1,2-diamine

Chemical Property:

Vapor Pressure:0.000457mmHg at 25°C
Melting Point:70 °C
Boiling Point:314.7°Cat760mmHg
PKA:3?+-.0.10(Predicted)
Flash Point:144.2°C
PSA：52.04000
Density:1.506g/cm³
LogP:3.39270
XLogP3:2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:214.01056
Heavy Atom Count:11
Complexity:140

Purity/Quality:

99%, ^*data from raw suppliers

5-Bromo-3,4-dimethylbenzene-1,2-diamine ^*data from reagent suppliers

Safty Information:

Pictogram(s): R20/21/22-36/37/38:;
Hazard Codes: Harmful:;
Statements: 20/21/22-36/37/38
Safety Statements: 22-24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C(=C1C)N)N)Br

Technology Process of 5-Bromo-3,4-dimethylbenzene-1,2-diamine

There total 5 articles about 5-Bromo-3,4-dimethylbenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₈H₇BrN₂O₄

: 107100-16-3
4-bromo-2,3-dimethyl-1,2-benzenediamine

Guidance literature:: With hydrogen; In tetrahydrofuran; water; at 120 ℃; for 20h; under 37503.8 Torr; chemoselective reaction;
DOI:10.1126/science.1242005

Reference yield: 87.0%

: 108485-13-8
4-bromo-2,3-dimethyl-6-nitroaniline

: 107100-16-3
4-bromo-2,3-dimethyl-1,2-benzenediamine

Guidance literature:: With ammonium hydroxide; sodium dithionite; In methanol; for 3h; Heating;

Reference yield:

: 59146-96-2
2,3-dimethyl-6-nitroaniline

: 107100-16-3
4-bromo-2,3-dimethyl-1,2-benzenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridinium bromide perbromide, AcOH / 0.5 h / Ambient temperature

2: 87 percent / 25percent aq. NH₃, sodium dithionite / methanol / 3 h / Heating

With ammonium hydroxide; sodium dithionite; pyridinium hydrobromide perbromide; acetic acid; In methanol;