1,4-Bis(beta-oxophenethyl)benzene

Base Information

Chemical Name:1,4-Bis(beta-oxophenethyl)benzene
CAS No.:24447-21-0
Molecular Formula:C₂₂H₁₈O₂
Molecular Weight:314.384
Hs Code.:
DSSTox Substance ID:DTXSID501270871
Nikkaji Number:J839.155F

Synonyms:Maybridge4_002577;Oprea1_680301;SCHEMBL7199268;DTXSID501270871;HMS1528F03;1,4-Bis(beta-oxophenethyl)benzene;IDI1_032455;2,2'-(1,4-Phenylene)bis[1-phenylethanone];BRD-K80855119-001-01-1;BRD-K80855119-001-02-9;24447-21-0

Suppliers and Price of 1,4-Bis(beta-oxophenethyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,4-Bis(beta-oxophenethyl)benzene

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:314.130679813
Heavy Atom Count:24
Complexity:368

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)CC2=CC=C(C=C2)CC(=O)C3=CC=CC=C3

Technology Process of 1,4-Bis(beta-oxophenethyl)benzene

There total 4 articles about 1,4-Bis(beta-oxophenethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 622-75-3
1,4-phenylenediacetonitrile

: potassium phenyltrifluoborate

: 24447-21-0
p-bis(phenacyl)benzene

Guidance literature:: With 1,10-Phenanthroline; water; palladium diacetate; trifluoroacetic acid; In 2-methyltetrahydrofuran; at 80 ℃; for 48h; Inert atmosphere; Schlenk technique;
DOI:10.3184/174751913X13730099043760

Reference yield: 40.0%

: p-bis(2-carboxy-2-hydroxy-2-phenylethyl)benzene

: 24447-21-0
p-bis(phenacyl)benzene

Guidance literature:: With (NMe₄)Co(III)Me₂opba*2H₂O*CH₃CN; oxygen; pivalaldehyde; In acetonitrile; for 3h;
DOI:10.1016/S0040-4020(00)01097-8

Reference yield:

: p-bis(2-hydroxy-2-methoxycarbonyl-2-phenylethyl)benzene

: 24447-21-0
p-bis(phenacyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol / 20 °C

2: 40 percent / (NMe₄)Co(III)Me₂opba*2H₂O*CH₃CN; pivalaldehyde; O₂ / acetonitrile / 3 h

With potassium hydroxide; (NMe₄)Co(III)Me₂opba*2H₂O*CH₃CN; oxygen; pivalaldehyde; In ethanol; acetonitrile;
DOI:10.1016/S0040-4020(00)01097-8