(5aα,7β,8aα)-7-(4-nitrophenylcarbonyloxy)-tetrahydrocyclopenta[f]-1,3,5-trioxepane

Base Information

• Chemical Name: (5aα,7β,8aα)-7-(4-nitrophenylcarbonyloxy)-tetrahydrocyclopenta[f]-1,3,5-trioxepane
• CAS No.: 1089180-36-8
• Molecular Formula: C₁₄H₁₅NO₈
• Molecular Weight: 325.275

Synonyms:(5aα,7β,8aα)-7-(4-nitrophenylcarbonyloxy)-tetrahydrocyclopenta[f]-1,3,5-trioxepane

Chemical Property of (5aα,7β,8aα)-7-(4-nitrophenylcarbonyloxy)-tetrahydrocyclopenta[f]-1,3,5-trioxepane

Chemical Property:

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Technology Process of (5aα,7β,8aα)-7-(4-nitrophenylcarbonyloxy)-tetrahydrocyclopenta[f]-1,3,5-trioxepane

There total 1 articles about (5aα,7β,8aα)-7-(4-nitrophenylcarbonyloxy)-tetrahydrocyclopenta[f]-1,3,5-trioxepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(5aα,7β,8aα)-7-hydroxytetrahydrocyclopenta[f]-1,3,5-trioxepane (1089180-31-3) + 4-Nitrophenyl chloroformate (7693-46-1) → (5aα,7β,8aα)-7-(4-nitrophenylcarbonyloxy)-tetrahydrocyclopenta[f]-1,3,5-trioxepane (1089180-36-8)

Guidance literature:

With 4-methyl-morpholine; In tetrahydrofuran; at 23 ℃; for 1h;

DOI:10.1039/b809178a

Reference yield:

(5aα,7β,8aα)-7-(4-nitrophenylcarbonyloxy)-tetrahydrocyclopenta[f]-1,3,5-trioxepane (1089180-36-8) + N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-N-isobutyl-4-methoxybenzenesulfonamide (159005-71-7) → (1'S,2'R)-{1'-benzyl-2'-hydroxy-3'-[isobutyl(4-methoxybenzenesulfonyl)amino]propyl}carbamic acid (5aα,7β,8aα)-tetrahydrocyclopenta[f]-1,3,5-trioxaepan-7-yl ester (1089180-39-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 24h;

DOI:10.1039/b809178a

upstream raw materials:

(5aα,7β,8aα)-7-hydroxytetrahydrocyclopenta[f]-1,3,5-trioxepane

4-Nitrophenyl chloroformate

Downstream raw materials:

(1'S,2'R)-{1'-benzyl-2'-hydroxy-3'-[isobutyl(4-methoxybenzenesulfonyl)amino]propyl}carbamic acid (5aα,7β,8aα)-tetrahydrocyclopenta[f]-1,3,5-trioxaepan-7-yl ester

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