3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane

Base Information

Chemical Name:3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane
CAS No.:612092-88-3
Molecular Formula:C₂₄H₃₈N₂O₃
Molecular Weight:402.577
Hs Code.:

Synonyms:3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane

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Chemical Property of 3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane

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Technology Process of 3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane

There total 3 articles about 3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 100-39-0
benzyl bromide

: 612092-87-2
3-tert-butyloxycarbonyl-7-(5-hydroxypentyl)-3,7-diazabicyclo[3.3.1]nonane

: 612092-88-3
3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0957-4166(03)00483-X

Reference yield:

: 612092-86-1
3-tert-butyloxycarbonyl-7-(5-hydroxypentyl)-9-oxo-3,7-diazabicyclo[3.3.1]nonane

: 612092-88-3
3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane

Guidance literature:: Multi-step reaction with 3 steps

1: TsNHNH₂ / ethanol / 3 h / Heating

2: 2.71 g / NaBH₄ / tetrahydrofuran; H₂O / 2 h / Heating

3: 93 percent / NaH; TBAI / tetrahydrofuran

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid hydrazide; In tetrahydrofuran; ethanol; water;
DOI:10.1016/S0957-4166(03)00483-X

Reference yield:

: C₂₄H₃₈N₄O₅S

: 612092-88-3
3-tert-butyloxycarbonyl-7-(5-benzyloxypentyl)-3,7-diazabicyclo[3.3.1]nonane

Guidance literature:: Multi-step reaction with 2 steps

1: 2.71 g / NaBH₄ / tetrahydrofuran; H₂O / 2 h / Heating

2: 93 percent / NaH; TBAI / tetrahydrofuran

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; water;
DOI:10.1016/S0957-4166(03)00483-X