1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine

Base Information

Chemical Name:1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine
CAS No.:1457967-34-8
Molecular Formula:C₂₉H₄₄N₄
Molecular Weight:448.695
Hs Code.:

Synonyms:1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine

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Chemical Property of 1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine

Chemical Property:

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Technology Process of 1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine

There total 8 articles about 1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₄₆N₄O

: 1457967-34-8
1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine

Guidance literature:: With sodium hydroxide; In ethanol; water; for 18h; Reflux;
DOI:10.1039/c3ob40816g

Reference yield:

: 2587-02-2
2,6-dichloro-[4]pyridylamine

: 1457967-34-8
1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid; nitric acid / 1 h / 0 - 20 °C

2.1: sulfuric acid / 0.5 h / 90 °C

3.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3.2: 2 h / 20 °C

4.1: triethylamine / dichloromethane / 48 h / Reflux

5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / water; 1,4-dioxane / 18 h / 90 °C / Inert atmosphere; Sealed tube

6.1: zinc; ammonium formate / methanol / 0.17 h / 20 °C

7.1: triethylamine / tetrahydrofuran / 1 h / Reflux

8.1: sodium hydroxide / ethanol; water / 18 h / Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; nitric acid; ammonium formate; sodium hydride; caesium carbonate; triethylamine; sodium hydroxide; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; 5.1: |Suzuki Coupling;
DOI:10.1039/c3ob40816g

Reference yield:

: 2897-43-0
2,6-dichloro-3-nitropyridin-4-amine

: 1457967-34-8
1-benzyl-2,6-dibutyl-N-(2,4,4-trimethylpentan-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 2 h / 20 °C

2.1: triethylamine / dichloromethane / 48 h / Reflux

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / water; 1,4-dioxane / 18 h / 90 °C / Inert atmosphere; Sealed tube

4.1: zinc; ammonium formate / methanol / 0.17 h / 20 °C

5.1: triethylamine / tetrahydrofuran / 1 h / Reflux

6.1: sodium hydroxide / ethanol; water / 18 h / Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium formate; sodium hydride; caesium carbonate; triethylamine; sodium hydroxide; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; 3.1: |Suzuki Coupling;
DOI:10.1039/c3ob40816g