N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester

Base Information

Chemical Name:N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester
CAS No.:148715-94-0
Molecular Formula:C₄₀H₄₆N₅O₈PS
Molecular Weight:787.874
Hs Code.:

Synonyms:N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester

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Chemical Property of N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester

Chemical Property:

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Technology Process of N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester

There total 11 articles about N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3417-91-2
L-tyrosine methyl ester HCl

: 148715-94-0
N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / N-methylmorpholine / CH₂Cl₂ / 1.) 5 deg C, 1 h, 2.) to r. t., 1 h

2: 90 percent / aq. NaHCO₃ / ethyl acetate

3: N-methylmorpholine / CH₂Cl₂ / 0.25 h / -5 °C

4: N-methylmorpholine, 2,6-luditine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; sodium hydrogencarbonate; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 2491-18-1
(S)-methyl 2-amino-4-(methylthio)butanoate hydrochloride

: 148715-94-0
N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: N-methylmorpholine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) to r. t., 1 h

2: HCl / methanol / 2 h

3: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

4: 86 percent / HCl / methanol / 0.5 h / 35 °C

5: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

6: HCl / methanol / 0.5 h / 35 °C

7: N-methylmorpholine, 2,6-luditine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 22248-60-8
L-phenylalanyl-L-methionine methyl ester

: 148715-94-0
N-(diphenylphosphinoyl)tyrosylglycylglycylphenylalanylmethionine methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

2: 86 percent / HCl / methanol / 0.5 h / 35 °C

3: N-methylmorpholine, 2,6-lutidine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

4: HCl / methanol / 0.5 h / 35 °C

5: N-methylmorpholine, 2,6-luditine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; In methanol; dichloromethane; N,N-dimethyl-formamide;