N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide

Base Information

Chemical Name:N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide
CAS No.:1586823-20-2
Molecular Formula:C₂₃H₁₈N₄O₄S
Molecular Weight:446.486
Hs Code.:

Synonyms:N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide

Chemical Property:

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Technology Process of N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide

There total 4 articles about N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1586822-28-7
C₁₆H₁₄N₂O₅S

: 873-74-5
4-Aminobenzonitrile

: 1586823-20-2
N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2014.02.003

Reference yield: 54.0%

: 1586823-20-2
N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

Reference yield:

: 50803-29-7
3-chlorosulfonyl-4-methoxybenzoic acid

: 1586823-20-2
N-(4-cyanophenyl)-3-(N-(4-cyanophenyl)-N-methylsulfamoyl)-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / ethyl acetate / 0 - 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With pyridine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2014.02.003