2-benzenesulfonylpent-4-enoic acid {5-[(2-benzenesulfonylpent-4-enoyl)-benzyloxyamino]pentyl}benzyloxyamide

Base Information

• Chemical Name: 2-benzenesulfonylpent-4-enoic acid {5-[(2-benzenesulfonylpent-4-enoyl)-benzyloxyamino]pentyl}benzyloxyamide
• CAS No.: 1094165-01-1
• Molecular Formula: C₄₁H₄₆N₂O₈S₂
• Molecular Weight: 758.957
• Mol file: 1094165-01-1.mol

Synonyms:2-benzenesulfonylpent-4-enoic acid {5-[(2-benzenesulfonylpent-4-enoyl)-benzyloxyamino]pentyl}benzyloxyamide

Chemical Property of 2-benzenesulfonylpent-4-enoic acid {5-[(2-benzenesulfonylpent-4-enoyl)-benzyloxyamino]pentyl}benzyloxyamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-benzenesulfonylpent-4-enoic acid {5-[(2-benzenesulfonylpent-4-enoyl)-benzyloxyamino]pentyl}benzyloxyamide

There total 1 articles about 2-benzenesulfonylpent-4-enoic acid {5-[(2-benzenesulfonylpent-4-enoyl)-benzyloxyamino]pentyl}benzyloxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.8%

N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl (1094164-87-0) + (but-3-en-1-ylsulfonyl)benzene (67100-44-1) → 2-benzenesulfonylpent-4-enoic acid {5-[(2-benzenesulfonylpent-4-enoyl)-benzyloxyamino]pentyl}benzyloxyamide (1094165-01-1)

Guidance literature:

(but-3-en-1-ylsulfonyl)benzene; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With water; acetic acid; In tetrahydrofuran;

DOI:10.1021/jo802410u

upstream raw materials:

N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

(but-3-en-1-ylsulfonyl)benzene