2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone

Base Information

Chemical Name:2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone
CAS No.:193964-27-1
Molecular Formula:C₂₄H₂₀O₃S
Molecular Weight:388.487
Hs Code.:

Synonyms:2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone

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Chemical Property of 2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone

Chemical Property:

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Technology Process of 2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone

There total 4 articles about 2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: aq KF

: 1461-25-2
tetra-n-butyltin(IV)

: 193964-26-0
2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-bromo-4-methoxyphenyl ketone

: 193964-27-1
2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone

Guidance literature:: SiO₂; tetrakis(triphenylphosphine)palladium ⁽⁰⁾; In diethyl ether; ethyl acetate; toluene;

Reference yield:

: 594-27-4
tetramethylstannane

: 193964-26-0
2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-bromo-4-methoxyphenyl ketone

: 193964-27-1
2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 130 ℃; for 4h;
DOI:10.1016/S0960-894X(98)00447-8

Reference yield:

: 27884-09-9
2-(4-methoxyphenyl)benzo[b]thiophene

: 193964-27-1
2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / TiCl₄ / 1,2-dichloro-ethane / 3 h

2: Pd(Ph₃P)4 / toluene / 4 h / 130 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; titanium tetrachloride; In 1,2-dichloro-ethane; toluene;
DOI:10.1016/S0960-894X(98)00447-8