2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone

Base Information

Chemical Name:2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone
CAS No.:193964-28-2
Molecular Formula:C₂₂H₁₆O₃S
Molecular Weight:360.433
Hs Code.:

Synonyms:2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone

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Chemical Property of 2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone

Chemical Property:

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Technology Process of 2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone

There total 4 articles about 2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 193964-27-1
2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-methoxyphenyl ketone

: 193964-28-2
2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone

Guidance literature:: With aluminium trichloride; ethanethiol; In 1,2-dichloro-ethane; for 16h;
DOI:10.1016/S0960-894X(98)00447-8

Reference yield:

: 193964-26-0
2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 3-bromo-4-methoxyphenyl ketone

: 193964-28-2
2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(Ph₃P)4 / toluene / 4 h / 130 °C

2: EtSH, AlCl₃ / 1,2-dichloro-ethane / 16 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; aluminium trichloride; ethanethiol; In 1,2-dichloro-ethane; toluene;
DOI:10.1016/S0960-894X(98)00447-8

Reference yield:

: 27884-09-9
2-(4-methoxyphenyl)benzo[b]thiophene

: 193964-28-2
2-(4-hydroxyphenyl)benzo[b]thiophen-3-yl 3-methyl-4-hydroxyphenyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / TiCl₄ / 1,2-dichloro-ethane / 3 h

2: Pd(Ph₃P)4 / toluene / 4 h / 130 °C

3: EtSH, AlCl₃ / 1,2-dichloro-ethane / 16 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; aluminium trichloride; titanium tetrachloride; ethanethiol; In 1,2-dichloro-ethane; toluene;
DOI:10.1016/S0960-894X(98)00447-8