1-(4-(4,5-dihydro-1H-pyrazol-1-yl)phenylsulfonyl)-4-methyl-1,2,3,4-tetrahydroquinoxaline

Base Information

Chemical Name:1-(4-(4,5-dihydro-1H-pyrazol-1-yl)phenylsulfonyl)-4-methyl-1,2,3,4-tetrahydroquinoxaline
CAS No.:1448427-11-9
Molecular Formula:C₁₈H₂₀N₄O₂S
Molecular Weight:356.448
Hs Code.:

Synonyms:1-(4-(4,5-dihydro-1H-pyrazol-1-yl)phenylsulfonyl)-4-methyl-1,2,3,4-tetrahydroquinoxaline

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Chemical Property of 1-(4-(4,5-dihydro-1H-pyrazol-1-yl)phenylsulfonyl)-4-methyl-1,2,3,4-tetrahydroquinoxaline

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Technology Process of 1-(4-(4,5-dihydro-1H-pyrazol-1-yl)phenylsulfonyl)-4-methyl-1,2,3,4-tetrahydroquinoxaline

There total 2 articles about 1-(4-(4,5-dihydro-1H-pyrazol-1-yl)phenylsulfonyl)-4-methyl-1,2,3,4-tetrahydroquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36438-97-8
1-methyl-1,2,3,4-tetrahydroquinoxaline

: C₉H₉ClN₂O₂S

: 1448427-11-9
1-(4-(4,5-dihydro-1H-pyrazol-1-yl)phenylsulfonyl)-4-methyl-1,2,3,4-tetrahydroquinoxaline

Guidance literature:: With triethylamine; In acetonitrile; at 130 ℃; for 0.5h; Sealed tube;
DOI:10.1016/j.bmc.2018.07.042

Reference yield:

: 936-53-8
1-phenyl-4,5-dihydro-1H-pyrazole

: 1448427-11-9
1-(4-(4,5-dihydro-1H-pyrazol-1-yl)phenylsulfonyl)-4-methyl-1,2,3,4-tetrahydroquinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / 15 h

2: triethylamine / acetonitrile / 0.5 h / 130 °C / Sealed tube

With chlorosulfonic acid; triethylamine; In acetonitrile;
DOI:10.1016/j.bmc.2018.07.042