C₁₈H₁₈O₂

Base Information

Chemical Name:C₁₈H₁₈O₂
CAS No.:1615201-86-9
Molecular Formula:C₁₈H₁₈O₂
Molecular Weight:266.34
Hs Code.:

C<sub>18</sub>H<sub>18</sub>O<sub>2</sub>

Synonyms:C₁₈H₁₈O₂

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Chemical Property of C₁₈H₁₈O₂

Chemical Property:

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Technology Process of C₁₈H₁₈O₂

There total 7 articles about C₁₈H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1615211-65-8
2-methoxy-3-(2-methyl-4-prop-1-ynylphenyl)bicyclo[3.2.1 ]oct-2-en-4-one

: 1615201-86-9
C₁₈H₁₈O₂

Guidance literature:: With hydrogenchloride; In water; acetone; at 120 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 13290-74-9
1-chloro-2-methyl-4-nitrobenzene

: 1615201-86-9
C₁₈H₁₈O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: XPhos; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,2-dimethoxyethane / 1 h / 160 °C / Microwave irradiation

2.1: 5%-palladium/activated carbon; hydrogen / ethanol; ethyl acetate / 8 h / 20 °C / 3000.3 Torr / Inert atmosphere

3.1: hydrogen bromide; sodium nitrite / water; ethanol / 1 h / 0 °C / Inert atmosphere

3.2: 20 h / 0 - 20 °C / Inert atmosphere

4.1: potassium carbonate / acetone / 21 h / 20 °C

5.1: copper(l) iodide; cesium fluoride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 0.5 h / 110 °C / Inert atmosphere; Microwave irradiation

6.1: hydrogenchloride / water; acetone / 0.17 h / 120 °C / Microwave irradiation

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; 5%-palladium/activated carbon; hydrogen bromide; hydrogen; potassium carbonate; cesium fluoride; sodium nitrite; XPhos; In 1,2-dimethoxyethane; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; acetone;

Reference yield:

: 3-(4-bromo-2-methylphenyl)bicyclo[3.2.1]octane-2,4-dione

: 1615201-86-9
C₁₈H₁₈O₂

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 21 h / 20 °C

2: copper(l) iodide; cesium fluoride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 0.5 h / 110 °C / Inert atmosphere; Microwave irradiation

3: hydrogenchloride / water; acetone / 0.17 h / 120 °C / Microwave irradiation

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; potassium carbonate; cesium fluoride; In water; N,N-dimethyl-formamide; acetone;