1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone

Base Information

Chemical Name:1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone
CAS No.:117671-93-9
Molecular Formula:C₁₄H₁₆O₃S₂
Molecular Weight:296.411
Hs Code.:

Synonyms:1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone

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Chemical Property of 1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone

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Technology Process of 1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone

There total 1 articles about 1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 89812-52-2
(E)-5-(4-methoxyphenyl)-1,1-bis(methylthio)-penta-1,4-dien-3-one

: 117671-93-9
1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In methanol; for 6h; Ambient temperature;
DOI:10.1055/s-1987-28112

Reference yield: 88.0%

: 117671-93-9
1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone

: 117672-01-2
(Z)-3-Hydroxy-2-(4-methoxy-phenyl)-5,5-bis-methylsulfanyl-penta-2,4-dienal

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; for 5h; Heating;
DOI:10.1055/s-1987-28112

Reference yield:

: 117671-93-9
1-[(2S,3R)-3-(4-Methoxy-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone

: 117672-09-0
5-(4-Methoxy-phenyl)-2-methylsulfanyl-pyran-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / BF₃*Et₂O / tetrahydrofuran / 5 h / Heating

2: 73 percent / acetic acid; ethanol / 5 h / Heating

With boron trifluoride diethyl etherate; In tetrahydrofuran; ethanol; acetic acid;
DOI:10.1055/s-1987-28112