methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate

Base Information

• Chemical Name: methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate
• CAS No.: 860264-48-8
• Molecular Formula: C₅₃H₆₂N₂O₁₀
• Molecular Weight: 887.083

Synonyms:methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate

Chemical Property of methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate

There total 2 articles about methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconic acid (860264-47-7) + diazomethane (186581-53-3,908094-01-9,334-88-3) → methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate (860264-48-8)

Guidance literature:

In methanol; diethyl ether; at 0 ℃; for 0.166667h;

DOI:10.1021/jo050494o

Reference yield: 84.0%

methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undec-3-enoate → methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate (860264-48-8)

Guidance literature:

With sodium acetate; toluene-4-sulfonic acid hydrazide; In 1,2-dimethoxyethane; at 85 ℃;

DOI:10.1021/jo050494o

Reference yield:

methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate (860264-48-8) → 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconic acid (860264-47-7)

Guidance literature:

With sodium hydroxide; In ethanol; at 20 ℃; for 14h;

DOI:10.1021/jo050494o

upstream raw materials:

6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconic acid

diazomethane

Downstream raw materials:

6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconic acid

(2S,3S,4R,5S,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-[(S)-4-tert-butoxycarbonylamino-4-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-butyl]-piperidine-1-carboxylic acid benzyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 860264-48-8 methyl 6,10-anhydro-7,8,9,11-tetra-O-benzyl-6-N-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-2,3,4,5,6-pentadeoxy-L-erythro-L-galacto-undeconate

Send

Send

Metric Ton KG G Pound L ML

Send

Send