N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol

Base Information

Chemical Name:N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol
CAS No.:137591-95-8
Molecular Formula:C₂₉H₃₅N₃O₂
Molecular Weight:457.616
Hs Code.:

Synonyms:N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol

Suppliers and Price of N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol

Chemical Property:

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Technology Process of N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol

There total 5 articles about N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 137591-94-7
2-Pyridyl--indolylketoxim

: 137591-95-8
N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol

Guidance literature:: With ammonium hydroxide; zinc; In ethanol; for 5h; Heating;
DOI:10.1002/ardp.2503241003

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 137591-95-8
N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) NaH / 1) DMF, 0 deg C, 1 h 2) 0 deg C, 1 h 3) r.t., 3 h

2: 1) Lithiumdiisopropylamid / 1) THF, -78 deg C, 30 min 2) THF, -78 deg C, 10 h 3) r.t., 10 h

3: 91 percent / NH₂OH*HCl, NaOH / ethanol; H₂O / 12 h / Heating

4: 45 percent / Zn, 25percent NH₃ / ethanol / 5 h / Heating

With ammonium hydroxide; sodium hydroxide; hydroxylamine hydrochloride; sodium hydride; zinc; lithium diisopropyl amide; In ethanol; water;
DOI:10.1002/ardp.2503241003

Reference yield:

: 21086-33-9
2-bromo-1-(4-methoxyphenyl)-1-propanone

: 137591-95-8
N-<7-(2-Pyridyl)-7-aminoheptyl>-5-methoxy-3-methyl-2-(4-methoxyphenyl)-indol

Guidance literature:: Multi-step reaction with 5 steps

1: 41 percent / N,N-Dimethylanilin / xylene / 2 h / 180 °C

2: 1) NaH / 1) DMF, 0 deg C, 1 h 2) 0 deg C, 1 h 3) r.t., 3 h

3: 1) Lithiumdiisopropylamid / 1) THF, -78 deg C, 30 min 2) THF, -78 deg C, 10 h 3) r.t., 10 h

4: 91 percent / NH₂OH*HCl, NaOH / ethanol; H₂O / 12 h / Heating

5: 45 percent / Zn, 25percent NH₃ / ethanol / 5 h / Heating

With ammonium hydroxide; sodium hydroxide; hydroxylamine hydrochloride; sodium hydride; N,N-dimethyl-aniline; zinc; lithium diisopropyl amide; In ethanol; water; xylene;
DOI:10.1002/ardp.2503241003