1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol

Base Information

Chemical Name:1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol
CAS No.:104865-71-6
Molecular Formula:C₂₇H₂₈O₅S₂
Molecular Weight:496.648
Hs Code.:

Synonyms:1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol

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Chemical Property of 1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol

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Technology Process of 1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol

There total 1 articles about 1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 56579-86-3
2-(3,4-methylenedioxyphenyl)-1,3-dithiane

: 56879-12-0
1-(4-(benzyloxy)-2-methoxyphenyl)ethanone

: 104865-71-6
1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -70 - -20 ℃; for 1h;
DOI:10.1016/S0040-4039(00)94967-0

Reference yield: 78.0%

: 104865-71-6
1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol

: 104865-72-7
4-(2-Benzo[1,3]dioxol-5-yl-1-methyl-ethyl)-3-methoxy-phenol

Guidance literature:: With nickel; In 1,4-dioxane; for 20h; Heating;
DOI:10.1016/S0040-4039(00)94967-0

Reference yield:

: 104865-71-6
1-(2-Benzo[1,3]dioxol-5-yl-[1,3]dithian-2-yl)-1-(4-benzyloxy-2-methoxy-phenyl)-ethanol

: 28178-92-9,104973-90-2
futoquinol

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / Raney Ni / dioxane / 20 h / Heating

2: 1.) K₂CO₃ / 1.) acetone, reflux, 11 h, 2.) 125 grad C, 4 h

3: 51 percent / tetrahydrofuran / electrolyzis, glassy carbon anode, platinum cathode

4: 72 percent / DDQ / benzene / 24 h / Heating

With nickel; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; benzene;
DOI:10.1016/S0040-4039(00)94967-0