2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole

Base Information

Chemical Name:2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole
CAS No.:1402592-67-9
Molecular Formula:C₅₈H₅₁N₃O₄
Molecular Weight:854.061
Hs Code.:

Synonyms:2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole

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Chemical Property of 2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole

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Technology Process of 2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole

There total 4 articles about 2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 16200-52-5
3,4-diethyl-1H-pyrrole

: 1402592-64-6
benzyl 5-acetoxymethyl-3,4-diphenylpyrrole-2-carboxylate

: 1402592-67-9
2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole

Guidance literature:: With toluene-4-sulfonic acid; In isopropyl alcohol; for 16h; Reflux;
DOI:10.1021/jo301945f

Reference yield:

: 60317-41-1
ethyl 2-(hydroxyimino)-3-oxo-3-phenylpropanoate

: 1402592-67-9
2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; zinc; sodium acetate / 0.5 h / 70 - 120 °C

2: sodium phenyl-methanolate / 1.58 h / 20 - 230 °C

3: acetic acid; lead(IV) tetraacetate / 16 h / 20 °C

4: toluene-4-sulfonic acid / isopropyl alcohol / 16 h / Reflux

With sodium acetate; lead(IV) tetraacetate; toluene-4-sulfonic acid; acetic acid; sodium phenyl-methanolate; zinc; In isopropyl alcohol; 1: |Knorr Pyrrole Synthesis;
DOI:10.1021/jo301945f

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 1402592-67-9
2,5-bis(5-benzyloxycarbonyl-3,4-diphenyl-2-pyrrolylmethyl)-3,4-diethylpyrrole

Guidance literature:: Multi-step reaction with 5 steps

1: sodium nitrite; acetic acid / water / 15 - 20 °C

2: acetic acid; zinc; sodium acetate / 0.5 h / 70 - 120 °C

3: sodium phenyl-methanolate / 1.58 h / 20 - 230 °C

4: acetic acid; lead(IV) tetraacetate / 16 h / 20 °C

5: toluene-4-sulfonic acid / isopropyl alcohol / 16 h / Reflux

With sodium acetate; lead(IV) tetraacetate; toluene-4-sulfonic acid; acetic acid; sodium phenyl-methanolate; zinc; sodium nitrite; In water; isopropyl alcohol; 2: |Knorr Pyrrole Synthesis;
DOI:10.1021/jo301945f