diethyl 1,3-propylidenebis(4-oxybenzoate)

Base Information

Chemical Name:diethyl 1,3-propylidenebis(4-oxybenzoate)
CAS No.:69703-27-1
Molecular Formula:C₂₁H₂₄O₆
Molecular Weight:372.418
Hs Code.:

Synonyms:diethyl 1,3-propylidenebis(4-oxybenzoate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 1,3-propylidenebis(4-oxybenzoate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of diethyl 1,3-propylidenebis(4-oxybenzoate)

There total 2 articles about diethyl 1,3-propylidenebis(4-oxybenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.8%

: 120-47-8
Ethyl 4-hydroxybenzoate

: 109-64-8
1,3-dibromo-propane

: 69703-27-1
diethyl 1,3-propylidenebis(4-oxybenzoate)

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 75 ℃; for 48h;
DOI:10.1002/zaac.201000424

Reference yield:

: 69703-27-1
diethyl 1,3-propylidenebis(4-oxybenzoate)

Guidance literature:: p-Hydroxybenzoesaeure-aethylester, 1,3-Dibrom-propan, Na-aethylat, abs. EtOH, Kochen, 3-4 Std.;
DOI:10.1021/jo01061a047

Reference yield: 63.0%

: lanthanum(III) nitrate hexahydrate

: 69703-27-1
diethyl 1,3-propylidenebis(4-oxybenzoate)

: La₂(1,3-propylidenebis(4-oxybenzoate))2(1,3-propylidenebis(4-oxybenzoate)H)2

Guidance literature:: In ethanol; water; High Pressure; La nitrate and diethyl 1,3-propylidenebis(4-oxybenzoate) dissolved in mixt. of H2O and EtOH; heated in reactor at 140°C for 48 h; crystals collected, washed with EtOH and H2O, dried under reduced pressure at room temp.; elem. anal.;
DOI:10.1002/zaac.201000424