triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate

Base Information

Chemical Name:triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate
CAS No.:410074-25-8
Molecular Formula:C₄₅H₄₈O₆
Molecular Weight:684.873
Hs Code.:

Synonyms:triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate

Chemical Property:

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Technology Process of triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate

There total 5 articles about triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 100-39-0
benzyl bromide

: 410074-24-7
triethyl trindane-2,5,8-tricarboxylate

: triethyl cis,trans,trans-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate

: 410074-25-8
triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -30 - 20 ℃;

Reference yield:

: 100-39-0
benzyl bromide

: 410074-24-7
triethyl trindane-2,5,8-tricarboxylate

: 410074-25-8
triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate

Guidance literature:: triethyl trindane-2,5,8-tricarboxylate; With chromium⁽⁰⁾ hexacarbonyl; In tetrahydrofuran; dibutyl ether; for 72h; Heating;

benzyl bromide; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -30 - 20 ℃; for 4h; Further stages.;

Reference yield:

: 192826-85-0
hexaethyl trindane-2,2,5,5,8,8-hexacarboxylate

: 410074-25-8
triethyl cis,cis,cis-2,5,8-tribenzyltrindane-2,5,8-tricarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / aq. KOH / ethanol / 24 h / Heating

2: 98 percent / pyridine / 3 h / Heating

3: 94 percent / sulfuric acid / 5 h / Heating

4: 21 percent / LDA / tetrahydrofuran / -30 - 20 °C

With pyridine; potassium hydroxide; sulfuric acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol; 3: Fischer esterification;