4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene

Base Information

Chemical Name:4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene
CAS No.:1260369-14-9
Molecular Formula:C₂₇H₃₉N₅O₂Sn
Molecular Weight:584.349
Hs Code.:

Synonyms:4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene

Suppliers and Price of 4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene

There total 6 articles about 4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.8%

: 155720-49-3
4-(tributylstannyl)benzyl bromide

: 148869-67-4
4-nitrophenyl(1,2,4-triazol-4-yl)amine

: 1260369-14-9
4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 18h; Inert atmosphere;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1260369-14-9
4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / dimethyl sulfoxide / 20 °C

2: potassium carbonate / acetone / 18 h / 20 °C / Inert atmosphere

With potassium tert-butylate; potassium carbonate; In dimethyl sulfoxide; acetone;

Reference yield:

: 1461-22-9
tributyltin chloride

: 1260369-14-9
4-[(4H-1,2,4-Triazol-4-yl){4-(tributylstannyl)benzyl}amino]nitrobenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.83 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.58 h / 0 °C / Inert atmosphere

3.1: potassium bromide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

4.1: potassium carbonate / acetone / 18 h / 20 °C / Inert atmosphere

With n-butyllithium; potassium carbonate; triethylamine; potassium bromide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetone;