Technology Process of 4-(tributylstannyl)benzyl bromide
There total 4 articles about 4-(tributylstannyl)benzyl bromide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium bromide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 12h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.83 h / -78 °C / Inert atmosphere
1.2: 1.5 h / -78 - 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 0.58 h / 0 °C / Inert atmosphere
3.1: potassium bromide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
With
n-butyllithium; triethylamine; potassium bromide;
In
tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.83 h / -78 °C / Inert atmosphere
1.2: 1.5 h / -78 - 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 0.58 h / 0 °C / Inert atmosphere
3.1: potassium bromide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
With
n-butyllithium; triethylamine; potassium bromide;
In
tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
