1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate

Base Information

Chemical Name:1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate
CAS No.:1350724-78-5
Molecular Formula:C₂₆H₄₄O₆
Molecular Weight:452.632
Hs Code.:

Synonyms:1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate

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Chemical Property of 1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate

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Technology Process of 1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate

There total 4 articles about 1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1350724-36-5
C₃₃H₄₈O₆

: 1350724-78-5
1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate

Guidance literature:: With hydrogenchloride; In ethanol; water; at 80 - 90 ℃; for 3h;
DOI:10.1021/jm200529h

Reference yield:

: 17696-11-6
8-bromooctanoic acid

: 1350724-78-5
1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

3.1: hydrogenchloride / ethanol; water / 3 h / 80 - 90 °C

With hydrogenchloride; dmap; potassium fluoride; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; water; acetone;
DOI:10.1021/jm200529h

Reference yield:

: 60526-81-0
1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene

: 1350724-78-5
1,3-dihydroxypropan-2-yl 8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron tribromide / dichloromethane

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

3.1: hydrogenchloride / ethanol; water / 3 h / 80 - 90 °C

With hydrogenchloride; potassium fluoride; boron tribromide; potassium carbonate; In ethanol; dichloromethane; water; acetone;
DOI:10.1021/jm200529h