2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene

Base Information

Chemical Name:2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene
CAS No.:881199-40-2
Molecular Formula:C₂₅H₃₂O₅
Molecular Weight:412.526
Hs Code.:

Synonyms:2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene

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Technology Process of 2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene

There total 6 articles about 2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 66967-26-8
3,4-dimethoxy-2-(2-propenyl)phenol

: 634616-23-2
(2-allyl-3-isopropoxy-4-methoxyphenyl)methanol

: 881199-40-2
2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.3987/COM-05-10592

Reference yield:

: 621-59-0
isovanillin

: 881199-40-2
2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / K₂CO₃ / acetone / 8 h / Heating

2: 92 percent / 3 h / 180 °C

3: K₂CO₃ / acetone / 8 h / Heating

4: sodium borohydride / ethanol / 0.5 h / 20 °C

5: 55 percent / triphenylphosphane; diisopropyl diazenedicarboxylate / tetrahydrofuran / 12 h / 20 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; ethanol; acetone; 2: Claisen rearrangement / 5: Mitsunobu reaction;
DOI:10.3987/COM-05-10592

Reference yield:

: 18075-40-6
O-allylisovanillin

: 881199-40-2
2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / 3 h / 180 °C

2: K₂CO₃ / acetone / 8 h / Heating

3: sodium borohydride / ethanol / 0.5 h / 20 °C

4: 55 percent / triphenylphosphane; diisopropyl diazenedicarboxylate / tetrahydrofuran / 12 h / 20 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; ethanol; acetone; 1: Claisen rearrangement / 4: Mitsunobu reaction;
DOI:10.3987/COM-05-10592