(9,9-dimethyl-2-(10-phenylanthracen-9-yl)-9H-fluoren-7-yl)triphenylsilane

Base Information

Chemical Name:(9,9-dimethyl-2-(10-phenylanthracen-9-yl)-9H-fluoren-7-yl)triphenylsilane
CAS No.:1061350-61-5
Molecular Formula:C₅₃H₄₀Si
Molecular Weight:704.986
Hs Code.:

Synonyms:(9,9-dimethyl-2-(10-phenylanthracen-9-yl)-9H-fluoren-7-yl)triphenylsilane

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Chemical Property of (9,9-dimethyl-2-(10-phenylanthracen-9-yl)-9H-fluoren-7-yl)triphenylsilane

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Technology Process of (9,9-dimethyl-2-(10-phenylanthracen-9-yl)-9H-fluoren-7-yl)triphenylsilane

There total 2 articles about (9,9-dimethyl-2-(10-phenylanthracen-9-yl)-9H-fluoren-7-yl)triphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1335379-13-9
4,4,5,5-tetramethyl-2-(9,9-dimethyl-2-(triphenylsilyl)-9H-fluoren-7-yl)-1,3,2-dioxaborolane

: 23674-20-6
9-bromo-10-phenylanthracene

: 1061350-61-5
(9,9-dimethyl-2-(10-phenylanthracen-9-yl)-9H-fluoren-7-yl)triphenylsilane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In toluene; for 4h; Reflux; Inert atmosphere;
DOI:10.1039/c1jm12097b

Reference yield:

: 1061351-02-7
(2-bromo-9,9-dimethyl-9H-fluoren-7-yl)triphenylsilane

: 1061350-61-5
(9,9-dimethyl-2-(10-phenylanthracen-9-yl)-9H-fluoren-7-yl)triphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene / 4 h / Reflux; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; toluene; 2.1: Suzuki coupling;
DOI:10.1039/c1jm12097b