benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate

Base Information

Chemical Name:benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate
CAS No.:1352835-25-6
Molecular Formula:C₂₉H₃₀N₄O₅
Molecular Weight:514.581
Hs Code.:

Synonyms:benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate

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Chemical Property of benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate

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Technology Process of benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate

There total 6 articles about benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.7%

: 245117-18-4
4-(1H-indol-6-yl)morpholine

: 1352835-04-1
(E)-benzyl 2-methyl-3-(2-nitrovinyl)phenylcarbamate

: 1352835-25-6
benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate

Guidance literature:: at 137 ℃;

Reference yield:

: 5318-27-4
6-amino-1H-indole

: 1352835-25-6
benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / tert-butyl alcohol / 84 h / 100 °C / Sealed tube

2: 137 °C

With sodium carbonate; In tert-butyl alcohol;

Reference yield:

: 69022-35-1
2-methyl-3-amino-benzonitrile

: 1352835-25-6
benzyl 2-methyl-3-(1-(6-morpholino-1H-indol-3-yl)-2-nitroethyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / tetrahydrofuran / 72 h / 20 °C

2.1: diisobutylaluminium hydride / dichloromethane; tetrahydrofuran / 5.75 h / -78 - 20 °C

2.2: 0.5 h / 20 °C / Cooling with ice

3.1: ammonium acetate; acetic acid / 4.5 h / 90 °C

4.1: 137 °C

With ammonium acetate; diisobutylaluminium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; dichloromethane;