(R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide

Base Information

Chemical Name:(R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide
CAS No.:104576-57-0
Molecular Formula:3BrH*C₂₇H₄₀N₈O₅
Molecular Weight:799.401
Hs Code.:

Synonyms:(R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide

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Chemical Property of (R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide

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Technology Process of (R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide

There total 5 articles about (R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 102255-74-3
[(R)-5-tert-Butoxycarbonylamino-5-(2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethylcarbamoyl)-pentyl]-carbamic acid benzyl ester

: 104576-57-0
(R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid;
DOI:10.1021/jm00384a037

Reference yield:

: 55878-47-2
(R)-6-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-hexanoic acid

: 104576-57-0
(R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / DCC, HOBt / dimethylformamide

2: 83 percent / 30percent HBr / acetic acid

With hydrogen bromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00384a037

Reference yield:

: 96865-92-8
xanthine amine congener

: 104576-57-0
(R)-2,6-Diamino-hexanoic acid (2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-amide; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / DCC, HOBt / dimethylformamide

2: 83 percent / 30percent HBr / acetic acid

With hydrogen bromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00384a037