N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide

Base Information

• Chemical Name: N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide
• CAS No.: 1333376-87-6
• Molecular Formula: C₆₄H₆₄N₄O₈
• Molecular Weight: 1017.23

Synonyms:N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide

Chemical Property of N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide

Chemical Property:

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Technology Process of N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide

There total 4 articles about N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

pyrrolidine (123-75-1) + N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid dianhydride (1333376-86-5) → N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide (1333376-87-6)

Guidance literature:

at 55 ℃; for 24h; Inert atmosphere;

DOI:10.1002/ejoc.201100519

Reference yield:

(S)-3-amino-1-(4,4’-dimethoxytriphenylmethyl)-2-propanediol → N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide (1333376-87-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sulfuric acid / 1 h / 20 °C / Inert atmosphere

1.2: 0.75 h / 20 - 85 °C / Inert atmosphere

2.1: 24 h / 55 °C / Inert atmosphere

With sulfuric acid;

DOI:10.1002/ejoc.201100519

Reference yield:

2-Ethylhexylamine (104-75-6) → N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide (1333376-87-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sulfuric acid / 1 h / 20 °C / Inert atmosphere

1.2: 0.75 h / 20 - 85 °C / Inert atmosphere

2.1: 24 h / 55 °C / Inert atmosphere

With sulfuric acid;

DOI:10.1002/ejoc.201100519

upstream raw materials:

pyrrolidine

N-(2-ethylhexyl)-N'-[3-O-trityl-2-(S)-hydroxypropyl]-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid dianhydride

2-Ethylhexylamine

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

Downstream raw materials:

N-(2-ethylhexyl)-N'-{3-O-trityl-2-(S)-[(2-cyanoethoxy)-N,N-(diisopropylamino)phosphanyloxy]propyl}-1,7-dipyrrolidinylperylene-3,4:9,10-tetracarboxylic acid bisimide

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