(3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine

Base Information

Chemical Name:(3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine
CAS No.:165319-95-9
Molecular Formula:C₁₇H₁₈N₂O₆
Molecular Weight:346.34
Hs Code.:

Synonyms:(3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine

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Chemical Property of (3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine

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Technology Process of (3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine

There total 2 articles about (3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 165319-94-8
(tert-butyl-3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronate)-1-thymine

: 165319-95-9
(3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/S0957-4166(00)86288-6

Reference yield: 55.0%

: 63593-01-1
3'-O-benzyl-2'-deoxythymidine

: 165319-95-9
(3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine

Guidance literature:: With dipotassium peroxodisulfate; ruthenium(III) chloride trihydrate; potassium hydroxide; In water; at 20 ℃; for 4h;
DOI:10.1002/chem.201102816

Reference yield:

: 165319-95-9
(3'-O-benzyl-3'-deoxy-β-D-ribo-furanuronic acid)-1-thymine

: (3'-O-benzyloxy-6'-phenylsulphonyl-2',5',6'-trideoxy-β-D-ribo-5'-ene-hexofuranosyl)-1-thymine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-methylmorpholine, isobutyl chloroformate

2: 81 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 °C

With 4-methyl-morpholine; 3-chloro-benzenecarboperoxoic acid; isobutyl chloroformate; In dichloromethane;
DOI:10.1016/S0957-4166(00)86288-6