2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

Base Information

Chemical Name:2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene
CAS No.:79861-69-1
Molecular Formula:C₂₀H₃₄O
Molecular Weight:290.489
Hs Code.:

2-(4'-hydroxy-4'-methyl-Δ<sup>1',2'</sup>-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

Synonyms:2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

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Chemical Property of 2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

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Technology Process of 2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

There total 6 articles about 2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 917-64-6
methyl magnesium iodide

: 79861-68-0
2-(4'-oxo-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

: 79861-69-1
2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

Guidance literature:: In diethyl ether; 1) r.t., overnight 2) reflux, 2h;

Reference yield:

: 18445-88-0
(E)-5,9-dimethyldeca-4,8-dienal

: 79861-69-1
2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / tetrahydrofuran / 1) cooling, 2h 2) r.t., overnight 3) reflux, 2h

2: 50 percent / pyridinium chlorochromate / NaOAc / CH₂Cl₂ / 3 h / 10 °C

3: 1) NaH / THF, DMSO

4: 30 percent / Li / liq.NH₃ / EtOH / diethyl ether

5: 80 percent / diethyl ether / 1) r.t., overnight 2) reflux, 2h

With ethanol; ammonia; sodium acetate; lithium; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 79861-67-9
2-(p-methoxyphenyl)-6,10-dimethyl-1,5,9-undecatriene

: 79861-69-1
2-(4'-hydroxy-4'-methyl-Δ^1',2'-cyclohexenyl)-6,10-dimethyl-5,9-undecadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / Li / liq.NH₃ / EtOH / diethyl ether

2: 80 percent / diethyl ether / 1) r.t., overnight 2) reflux, 2h

With ethanol; ammonia; lithium; In diethyl ether;