C₁₂H₂₀ClNOSSi

Base Information

• Chemical Name: C₁₂H₂₀ClNOSSi
• CAS No.: 157736-03-3
• Molecular Formula: C₁₂H₂₀ClNOSSi
• Molecular Weight: 289.901
• Mol file: 157736-03-3.mol

Synonyms:C₁₂H₂₀ClNOSSi

Chemical Property of C₁₂H₂₀ClNOSSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₂H₂₀ClNOSSi

There total 2 articles about C₁₂H₂₀ClNOSSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1-Methyl-2-phenoxy-ethyl)-trimethylsilanyl-amine (157736-23-7) → C12H20ClNOSSi (157736-03-3)

Guidance literature:

With sulfur dichloride; triethylamine; In diethyl ether; 0.5 h, -10 degC, allowed to warm to 20 degC over 1 h;

DOI:10.1016/S0040-4039(00)77083-3

Reference yield:

1-methyl-2-phenoxyethylamine (35205-54-0) → C12H20ClNOSSi (157736-03-3)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / 16 h / 20 °C

2: Et₃N, SCl₂ / diethyl ether / 1.) -10 deg C, 0.5 h, 2.) -10 to 20 deg C, 0.5 h

With sulfur dichloride; triethylamine; In diethyl ether;

DOI:10.1039/p19960001825

Reference yield: 40.0%

2,3-dimethyl-buta-1,3-diene (513-81-5) + C12H20ClNOSSi (157736-03-3) → 2-(1-Methyl-2-phenoxyethyl)-4,5-dimethyl-3,6-dihydro-2H-1,2-thiazine (157736-14-6)

Guidance literature:

With silver fluoride; In acetonitrile; at 20 ℃; for 16h;

DOI:10.1039/p19960001825

upstream raw materials:

(1-Methyl-2-phenoxy-ethyl)-trimethylsilanyl-amine

1-methyl-2-phenoxyethylamine

Downstream raw materials:

2-(1-Methyl-2-phenoxyethyl)-4,5-dimethyl-3,6-dihydro-2H-1,2-thiazine