3-(R)-3-[2-(R)-2-methoxy-2-phenyl-2-trifluoromethyl]acetoxybutyric acid methyl ester

Base Information

Chemical Name:3-(R)-3-[2-(R)-2-methoxy-2-phenyl-2-trifluoromethyl]acetoxybutyric acid methyl ester
CAS No.:76904-87-5
Molecular Formula:C₁₅H₁₇F₃O₅
Molecular Weight:334.292
Hs Code.:

Synonyms:3-(R)-3-[2-(R)-2-methoxy-2-phenyl-2-trifluoromethyl]acetoxybutyric acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(R)-3-[2-(R)-2-methoxy-2-phenyl-2-trifluoromethyl]acetoxybutyric acid methyl ester

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Technology Process of 3-(R)-3-[2-(R)-2-methoxy-2-phenyl-2-trifluoromethyl]acetoxybutyric acid methyl ester

There total 2 articles about 3-(R)-3-[2-(R)-2-methoxy-2-phenyl-2-trifluoromethyl]acetoxybutyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 3976-69-0
Methyl (R)-3-hydroxybutyrate

: 76904-87-5
3-(R)-3-[2-(R)-2-methoxy-2-phenyl-2-trifluoromethyl]acetoxybutyric acid methyl ester

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.15227/orgsyn.071.0001

Reference yield:

: 20445-31-2
R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid

: 3976-69-0
Methyl (R)-3-hydroxybutyrate

: 76904-87-5
3-(R)-3-[2-(R)-2-methoxy-2-phenyl-2-trifluoromethyl]acetoxybutyric acid methyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86300-6