Technology Process of C21H34O4Si
There total 3 articles about C21H34O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C21H34O4Si;
With
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dimethyl sulfoxide; toluene;
With
sodium bis(2-methoxyethoxy)aluminium dihydride;
In
dichloromethane;
at -78 ℃;
DOI:10.1021/jo102033h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dmap; triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; toluene
2.2: -78 °C
With
dmap; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo102033h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dmap; triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; toluene
2.2: -78 °C
With
dmap; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo102033h