(2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid

Base Information

Chemical Name:(2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid
CAS No.:914939-81-4
Molecular Formula:C₂₈H₃₀N₂O₅
Molecular Weight:474.557
Hs Code.:

Synonyms:(2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid

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Chemical Property of (2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid

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Technology Process of (2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid

There total 4 articles about (2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 203585-49-3
phenylmethyl (4S)-4-{3-[bis(phenylmethyl)amino]-3-oxopropyl}-5-oxo-1,3-oxazolidine-3-carboxylate

: 914939-81-4
(2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/hlca.200690235

Reference yield:

: 1155-62-0
N-benzyloxycarbonyl-L-glutamic acid

: 914939-81-4
(2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: CSA / toluene / Heating

2: SOCl₂ / 0.25 h / Heating

3: CH₂Cl₂ / 0 - 20 °C

4: 90 percent / Et₃SiH; TFA / CH₂Cl₂

With triethylsilane; thionyl chloride; trifluoroacetic acid; camphor-10-sulfonic acid; In dichloromethane; toluene;
DOI:10.1002/hlca.200690235

Reference yield:

: 58456-26-1
(S)-4-<2'-(Chloroformyl)ethyl>-5-oxooxazolidin-3-carbonsaeure-benzylester

: 914939-81-4
(2S)-5-[bis(phenylmethyl)amino]-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)-5-oxopentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0 - 20 °C

2: 90 percent / Et₃SiH; TFA / CH₂Cl₂

With triethylsilane; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/hlca.200690235