(E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide

Base Information

Chemical Name:(E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide
CAS No.:1486515-58-5
Molecular Formula:C₁₆H₂₄FNO₂S
Molecular Weight:313.436
Hs Code.:

Synonyms:(E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide

Suppliers and Price of (E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide

There total 4 articles about (E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1486515-50-7
(E)-N-methyl-N-(1-tributylstannyl-oct-1-en-1-yl)tosylamide

: 1486515-58-5
(E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide

Guidance literature:: With silver trifluoromethanesulfonate; sodium hydrogencarbonate; Selectfluor; In acetone; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol4031028

Reference yield:

: 1007597-75-2
N,4-dimethyl-N-(oct-1-yn-1-yl)benzenesulfonamide

: 1486515-58-5
(E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydroquinone; tris(t-butyl isocyanide)tricarbonylmolybdenum(O); carbon monoxide / tetrahydrofuran / 55 °C / Schlenk technique

2: silver trifluoromethanesulfonate; Selectfluor; sodium hydrogencarbonate / acetone / 16 h / 20 °C / Inert atmosphere

With tris(t-butyl isocyanide)tricarbonylmolybdenum(O); carbon monoxide; silver trifluoromethanesulfonate; sodium hydrogencarbonate; Selectfluor; hydroquinone; In tetrahydrofuran; acetone;
DOI:10.1021/ol4031028

Reference yield:

: 629-05-0
n-octyne

: 1486515-58-5
(E)-N-(1-fluorooct-1-en-1-yl)-N-methyltosylamide

Guidance literature:: Multi-step reaction with 4 steps

1: silver nitrate; N-Bromosuccinimide / acetone / 20 °C

2: potassium carbonate; copper(II) sulfate; 1,10-Phenanthroline / toluene; water / 80 °C

3: hydroquinone; tris(t-butyl isocyanide)tricarbonylmolybdenum(O); carbon monoxide / tetrahydrofuran / 55 °C / Schlenk technique

4: silver trifluoromethanesulfonate; Selectfluor; sodium hydrogencarbonate / acetone / 16 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; 1,10-Phenanthroline; tris(t-butyl isocyanide)tricarbonylmolybdenum(O); carbon monoxide; silver trifluoromethanesulfonate; sodium hydrogencarbonate; potassium carbonate; silver nitrate; copper(II) sulfate; Selectfluor; hydroquinone; In tetrahydrofuran; water; acetone; toluene;
DOI:10.1021/ol4031028