(3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate

Base Information

Chemical Name:(3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate
CAS No.:624738-99-4
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

Synonyms:(3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate

Chemical Property:

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Technology Process of (3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate

There total 5 articles about (3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 31139-36-3
dibenzyl dicarbonate

: 624739-11-3
(3R,5E,αR)-methyl 3-(N-[α-methylbenzyl]amino)-hept-5-enoate

: 624738-99-4
(3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate

Guidance literature:: for 96h;
DOI:10.1039/b305740b

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 501-53-1,94274-21-2
benzyl chloroformate

: 100-51-6,185532-71-2
benzyl alcohol

: 624739-11-3
(3R,5E,αR)-methyl 3-(N-[α-methylbenzyl]amino)-hept-5-enoate

: 3459-92-5
DBC

: 624738-99-4
(3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate

Guidance literature:: Multistep reaction. Title compound not separated from byproducts;
DOI:10.1039/b404962d

Reference yield:

: 18261-30-8,32793-92-3,32793-93-4,40415-88-1,41792-07-8
(E,E)-methyl heptan-2,5-dieneoate

: 624738-99-4
(3R,5E,αR)-methyl 3-(N-[benzyloxycarbonyl]-N-[α-methylbenzyl]amino)hept-5-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / tetrahydrofuran / 2 h / -78 °C

2: 97 percent / Wilkinson's catalyst / acetonitrile; H₂O / 2 h / Heating

3: 88 percent / 96 h

Wilkinson's catalyst; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/b305740b