PdPtCoI(CO)3(dppm)2

Base Information

Chemical Name:PdPtCoI(CO)3(dppm)2
CAS No.:113132-12-0
Molecular Formula:C₅₃H₄₄CoIO₃P₄PdPt
Molecular Weight:1340.22
Hs Code.:

Synonyms:PdPtCoI(CO)3(dppm)2

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Chemical Property of PdPtCoI(CO)3(dppm)2

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Technology Process of PdPtCoI(CO)3(dppm)2

There total 5 articles about PdPtCoI(CO)3(dppm)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 113109-37-8
PdPtCo₂(CO)7(dppm)2

: 14878-26-3
potassium tetracarbonylcobaltate

: 113132-12-0
PdPtCoI(CO)3(dppm)2

Guidance literature:: With potassium iodide; In water; acetone; A soln. of KI in a mixt. of acetone and water was added to a stirred soln. of PdPtCo2(CO)7(dppm)2 in acetone. The dark green soln. immediately turned red. Stirred for 3 h.; The solvents were evapd. in vac.; The red solid residue was washed with water to remove K{Co(CO)4} and the excess of KI. Extn. with CH2Cl2 gave a red soln. After addn. of n-hexane, crystals were obtained at -20°C. Elem.anal.;

Reference yield: 68.0%

: 113109-37-8
PdPtCo₂(CO)7(dppm)2

: 68-05-3
tetraethylammonium iodide

: 113132-12-0
PdPtCoI(CO)3(dppm)2

Guidance literature:: In tetrahydrofuran; Solid NEt4I was added to a soln. of PdPtCo2(CO)7(dppm)2 in THF. The color of the react. mixt. turned from green to red.; The solvent was removed, and the resulting residue was washed with H2O and recrystd. from a mixt. of CH2Cl2 and n-C6H14. Purifn. by passage of its CH2Cl2 soln. through a silica gel column. Red fraction identified by IR.;