di-tert-butyl-4-formyl-2-nitrophenyl phosphate

Base Information

Chemical Name:di-tert-butyl-4-formyl-2-nitrophenyl phosphate
CAS No.:169565-39-3
Molecular Formula:C₁₅H₂₂NO₇P
Molecular Weight:359.316
Hs Code.:

Synonyms:di-tert-butyl-4-formyl-2-nitrophenyl phosphate

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Chemical Property of di-tert-butyl-4-formyl-2-nitrophenyl phosphate

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Technology Process of di-tert-butyl-4-formyl-2-nitrophenyl phosphate

There total 1 articles about di-tert-butyl-4-formyl-2-nitrophenyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59346-65-5
di-tert-butyl phosphorobromidate

: 3011-34-5
4-hydroxy-3-nitrobenzaldehyde

: 169565-39-3
di-tert-butyl-4-formyl-2-nitrophenyl phosphate

Guidance literature:: With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 0 - 20 ℃; for 1h;
DOI:10.1021/ja00150a002

Reference yield:

: 169565-39-3
di-tert-butyl-4-formyl-2-nitrophenyl phosphate

: 169565-40-6
di-tert-butyl-4-(hydroxymethyl)-2-nitrophenyl phosphate

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at -78 ℃; for 1h; Yield given;
DOI:10.1021/ja00150a002

Reference yield:

: 169565-39-3
di-tert-butyl-4-formyl-2-nitrophenyl phosphate

: Phosphoric acid mono-(4-fluoromethyl-2-nitro-phenyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / CH₂Cl₂; methanol / 1 h / -78 °C

2: 45 percent / diethylamino sulfurtrifluoride / CH₂Cl₂ / 1 h / 0 °C

3: trifluoromethanesulfonic acid / tetrahydrofuran / 16 h / Ambient temperature

With sodium tetrahydroborate; trifluorormethanesulfonic acid; diethylamino-sulfur trifluoride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja00150a002