(3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine

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Chemical Name:(3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine
CAS No.:903561-96-6
Molecular Formula:C₇₁H₅₆BrNO₆
Molecular Weight:1099.13
Hs Code.:

Synonyms:(3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine

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Chemical Property of (3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine

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Technology Process of (3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine

There total 14 articles about (3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 903561-96-6
(3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / K₂CO₃; 18-crown-6 / tetrahydrofuran / 12 h / Heating

2: 76 percent / K₂CO₃; 18-crown-6 / tetrahydrofuran / 12 h / Heating

3: 4-(dimethylamino)pyridine; triethylamine / tetrahydrofuran / 3 h / 20 °C

4: lithium bromide / tetrahydrofuran / Heating

With dmap; 18-crown-6 ether; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran;
DOI:10.1021/ol0608956

Reference yield:

: methanesulfonic acid 3-{3-benzyloxy-5-[3-(phenyl-pyren-1-yl-amino)-benzyloxy]-benzyloxy}-5-(3,5-bis-benzyloxy-benzyloxy)-benzyl ester

: 903561-96-6
(3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine

Guidance literature:: With lithium bromide; In tetrahydrofuran; Heating;
DOI:10.1021/ol0608956

Reference yield:

: methanesulfonic acid 3-(phenyl-pyren-1-yl-amino)-benzyl ester

: 903561-96-6
(3-{3-benzyloxy-5-[3-(3,5-bis-benzyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-phenoxymethyl}-phenyl)-phenyl-pyren-1-yl-amine

Guidance literature:: Multi-step reaction with 7 steps

1: lithium bromide / tetrahydrofuran / Heating

2: 80 percent / K₂CO₃; 18-crown-6 / tetrahydrofuran / 12 h / Heating

3: 4-(dimethylamino)pyridine; triethylamine / tetrahydrofuran / 3 h / 20 °C

4: lithium bromide / tetrahydrofuran / Heating

5: 76 percent / K₂CO₃; 18-crown-6 / tetrahydrofuran / 12 h / Heating

6: 4-(dimethylamino)pyridine; triethylamine / tetrahydrofuran / 3 h / 20 °C

7: lithium bromide / tetrahydrofuran / Heating

With dmap; 18-crown-6 ether; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran;
DOI:10.1021/ol0608956