<5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone

Base Information

Chemical Name:<5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone
CAS No.:129609-37-6
Molecular Formula:C₁₄H₁₂ClN₃O₂S
Molecular Weight:321.787
Hs Code.:

Synonyms:<5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone

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Chemical Property of <5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone

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Technology Process of <5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone

There total 7 articles about <5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: CH₂ Cl₂ -EtOAc

: 96938-79-3
5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazole-4-carbonyl chloride

: 129609-38-7
<5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(2,5-dihydro-4-hydroxy-3-thienyl)methanone

: 129609-37-6
<5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone

Guidance literature:: In diethyl ether; dichloromethane;

Reference yield:

: 75020-50-7
ethyl 1-benzyl-5-chloro-1H-1,2,3-triazole-4-carboxylate

: 129609-37-6
<5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: saponification according to J_. Heterocyclic Chem_., 22, 77-80 ⁽¹⁹⁸⁵⁾

2: according to J_. Heterocyclic Chem_., 22, 77-80 ⁽¹⁹⁸⁵⁾

3: 4.5 g / triethylamine / CH₂Cl₂ / 1) -30 deg C, 1 h, 2) 25 deg C

With triethylamine; In dichloromethane;

Reference yield:

: 15212-80-3
1-Benzyl-5-chloro-1H-1,2,3-triazole-4-carboxylic acid

: 129609-37-6
<5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazol-4-yl>(4,5-dihydro-3-hydroxy-2-thienyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: according to J_. Heterocyclic Chem_., 22, 77-80 ⁽¹⁹⁸⁵⁾

2: 4.5 g / triethylamine / CH₂Cl₂ / 1) -30 deg C, 1 h, 2) 25 deg C

With triethylamine; In dichloromethane;