ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate

Base Information

Chemical Name:ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate
CAS No.:924272-34-4
Molecular Formula:C₂₆H₂₅N₃O₅S
Molecular Weight:491.568
Hs Code.:

Synonyms:ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate

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Chemical Property of ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate

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Technology Process of ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate

There total 3 articles about ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 97651-29-1
ethyl 3-cyano-1,2-dihydro-4-p-methoxyphenyl-6-methyl-2-thioxopyridin-4-carboxylate

: 22303-36-2
N-(4-methoxyphenyl)-2-chloroacetamide

: 924272-34-4
ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate

Guidance literature:: With sodium acetate; In ethanol; for 2h; Heating;
DOI:10.1080/10426500601096369

Reference yield:

: 141-97-9
ethyl acetoacetate

: 924272-34-4
ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / Heating

2: 87 percent / sodium acetate trihydrate / ethanol / 2 h / Heating

With piperidine; sodium acetate; In ethanol;
DOI:10.1080/10426500601096369

Reference yield:

: 68029-57-2
2-cyano-3-(4-methoxyphenyl)thioacrylamide

: 924272-34-4
ethyl 5-cyano-6-({2-[(4-methoxyphenyl)amino]-2-oxoethyl}thio)-4-(4-methoxyphenyl)-2-methylnicotinate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / Heating

2: 87 percent / sodium acetate trihydrate / ethanol / 2 h / Heating

With piperidine; sodium acetate; In ethanol;
DOI:10.1080/10426500601096369