C₄₉H₆₅NO₁₃Si

Base Information

• Chemical Name: C₄₉H₆₅NO₁₃Si
• CAS No.: 651293-91-3
• Molecular Formula: C₄₉H₆₅NO₁₃Si
• Molecular Weight: 904.14
• Mol file: 651293-91-3.mol

Synonyms:C₄₉H₆₅NO₁₃Si

Chemical Property of C₄₉H₆₅NO₁₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₄₉H₆₅NO₁₃Si

There total 2 articles about C₄₉H₆₅NO₁₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

triethylsilyl chloride (994-30-9) + 10β-deacetylcephalomannine (76429-85-1,78479-12-6) → C49H65NO13Si (651293-91-3)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1002/ejoc.200300376

Reference yield:

cephalomannine (71610-00-9) → C49H65NO13Si (651293-91-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / aq. H₂O₂; NaHCO₃ / tetrahydrofuran / 24 h / 20 °C

2: 51 percent / imidazole / dimethylformamide / 1 h / 20 °C

With 1H-imidazole; dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.200300376

Reference yield: 89.0%

C49H65NO13Si (651293-91-3) → C49H63NO13Si

Guidance literature:

With copper diacetate; air; In methanol; for 24h;

DOI:10.1002/ejoc.200300376

upstream raw materials:

triethylsilyl chloride

10β-deacetylcephalomannine

cephalomannine

Refernces