2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide

Base Information

Chemical Name:2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide
CAS No.:134793-54-7
Molecular Formula:C₂₀H₁₅F₃N₆O₄S
Molecular Weight:492.438
Hs Code.:

Synonyms:2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide

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Chemical Property of 2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide

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Technology Process of 2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide

There total 4 articles about 2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 134793-40-1
3-thioxo-6-(2-trifluoroacetamidophenyl)-1,2,4-triazin-5(2H,4H)one

: 4791-23-5
N-chloroacetyl-N'-phenylurea

: 134793-54-7
2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide

Guidance literature:: With sodium hydroxide; In ethanol; for 6h; Heating;

Reference yield:

: 27161-64-4
6-(2’-aminophenyl)-3-thioxo-3,4-dihydro-1,2,4-triazin-5(2H)-one

: 134793-54-7
2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / piperidine / ethanol / 2 h / Heating

2: 60 percent / sodium hydroxide / ethanol / 6 h / Heating

With piperidine; sodium hydroxide; In ethanol;

Reference yield:

: 134793-40-1
3-thioxo-6-(2-trifluoroacetamidophenyl)-1,2,4-triazin-5(2H,4H)one

: 134793-54-7
2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 2 h / Heating

2: benzene / 4 h / Heating

In N,N-dimethyl-formamide; benzene;