2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide

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Chemical Name:2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide
CAS No.:134793-59-2
Molecular Formula:C₂₂H₁₅F₃N₆O₄S
Molecular Weight:516.46
Hs Code.:

Synonyms:2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide

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Chemical Property of 2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide

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Technology Process of 2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide

There total 3 articles about 2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 506-96-7
Acetyl bromide

: 134793-54-7
2-(6-trifluoroacetamidophenyl-1,2,4-triazin-5-one-3-yl)thio-N-(phenylamino)carbonyl acetamide

: 134793-59-2
2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide

Guidance literature:: With sodium ethanolate; In ethanol; for 3h; Heating;

Reference yield:

: 134793-40-1
3-thioxo-6-(2-trifluoroacetamidophenyl)-1,2,4-triazin-5(2H,4H)one

: 134793-59-2
2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / sodium hydroxide / ethanol / 6 h / Heating

2: 85 percent / sodium ethylate / ethanol / 3 h / Heating

With sodium hydroxide; sodium ethanolate; In ethanol;

Reference yield:

: 27161-64-4
6-(2’-aminophenyl)-3-thioxo-3,4-dihydro-1,2,4-triazin-5(2H)-one

: 134793-59-2
2,2,2-Trifluoro-N-{2-[3-(6-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylsulfanyl)-5-oxo-4,5-dihydro-[1,2,4]triazin-6-yl]-phenyl}-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / piperidine / ethanol / 2 h / Heating

2: 60 percent / sodium hydroxide / ethanol / 6 h / Heating

3: 85 percent / sodium ethylate / ethanol / 3 h / Heating

With piperidine; sodium hydroxide; sodium ethanolate; In ethanol;