(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate

Base Information

Chemical Name:(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate
CAS No.:170943-85-8
Molecular Formula:C₃₄H₅₀N₂O₄S
Molecular Weight:582.848
Hs Code.:

Synonyms:(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate

Chemical Property:

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Technology Process of (1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate

There total 5 articles about (1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 171038-15-6
(2R)-(1S,2R,4R)-10-(Dicyclohexylsulfamoyl)isobornyl 2-cyano-2-phenyl-4-pentenoate

: 170943-85-8
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; Ambient temperature;

Reference yield:

: 30698-30-7
methyl 2-cyano-2-phenylacetate

: 170943-85-8
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Me₃Al / 1.) toluene, hexane, RT, 30 min, 2.) toluene, hexane, 80 deg C, 8 h

2: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 1 h, 2.) THF, RT, 1 d

With N,N,N,N,N,N-hexamethylphosphoric triamide; trimethylaluminum; lithium diisopropyl amide;

Reference yield:

: 96303-88-7
(-)-10-dicyclohexylsulfamoyl-D-isoborneol

: 170943-85-8
(1S,2R,4R)-10-dicyclohexylsulfamoylisobornyl (2R)-2-phenyl-2-cyanopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Me₃Al / 1.) toluene, hexane, RT, 30 min, 2.) toluene, hexane, 80 deg C, 8 h

2: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 1 h, 2.) THF, RT, 1 d

With N,N,N,N,N,N-hexamethylphosphoric triamide; trimethylaluminum; lithium diisopropyl amide;